DECI NEWSLETTERS AND REPORTS


THE DECI REPORT - JANUARY 1997


ACOUSTIC EMISSION ANALYSIS OF A GRAPHITE-EPOXY HONEYCOMB PANEL


INTRODUCTION

Acoustic emission technology has been used very successfully over the past three decades for the testing of man lift vehicle booms, pressure vessels, and piping made from fiberglass composite materials. There is presently a great deal of interest in using AE technology for the testing of more exotic composite materials such as graphite-epoxy compositions. These materials have a high strength to weight ratio, a high elastic modulus, and are suitable for cryogenic applications.



This report shows the results of recent acoustic emission experimental work on a graphite-epoxy honeycomb panel of the type used for aircraft and space applications. The overall thickness of the panel was 0.875 in. (21.9mm) with 0.070 in. (1.8mm) graphite-epoxy panels covering the top and bottom surfaces of the honeycomb material. The panel was 20 inches (500mm) X 32 inches (800mm) in size. The purpose of this experimental program was the following:

1. Compare the SE9125-MI "false aperture" transducer performance with the SE1000-HI high fidelity transducer for composite applications.
2. Measure the velocity and attenuation of the graphite-epoxy material.
3. Determine the effectiveness of using a waveguide with a sharp point for composite applications.
4. Determine whether or not one can effectively measure sources of AE on one side of the panel when the transducers are mounted on the opposite side.

PROCEDURE

The general procedure was to couple a trigger transducer at the edge and midpoint of one side of the panel with petroleum jelly as shown in figure 1. The output of this transducer was used to trigger the sweep of a digital oscilloscope. Three data transducers, the SE1000-HI , the SE1000-HI with 4.5 inch (113mm) waveguide with pointed end, and the SE9125-MI were used for the results given in this report. These transducers contain internal electronics with approximately 10dB of gain and are designed to drive hundreds of feet of 50 ohm cable without loss of signal. The signals from each transducer were amplified by 40dB by a preamplifier containing a 20Khz hipass filter before being displayed by the digital oscilloscope. These transducers were located at different distances from the pencil lead breaks in order to measure velocity and attenuation of the different types of waves produced in the panel. Out-of-plane (OOP) pencil lead breaks were made on the top and bottom surfaces with the pencil held parallel with the plane of the panel. In-plane (IP) pencil lead breaks were made on the center edge of the panel again with the pencil held parallel to the plane of the panel. Holding the pencil lead parallel to the plane of the panel is necessary in order to prevent mixed modes from being input into the panel. The data transducers were coupled to the panel with petroleum jelly. There was no couplant used for the pointed waveguide.

EXPERIMENTAL RESULTS

Figure 2 shows a comparison between the SE9125-MI and the SE1000-HI transducers when placed at different distances from the IP pencil lead break at the edge of the panel. Note that both the extensional and shear wave from this IP source is detected by both transducers, with a minimal amount of the low frequency flexural wave component present. This is due to the attempt to break the pencil lead as closely as possible at the center edge of the top panel. The arrival of the shear wave (second large signal) is shown clearly by the data at the 8 inch position for both transducers and has a very low value of approximately 53,300in/sec. (1,330m/sec.) The extensional velocity is approximately 200,000in/sec. (5,000m/sec.) which is quite high for a composite material.



Note the change in the vertical scale for the three distances. If one utilizes the data for the extensional wave in figure 2(e) and 2(f), an order of magnitude change in amplitude is observed for 8 inches (200mm) of travel indicating an approximate attenuation in this particular panel of 2.5dB/inch (.1db/mm) for an IP signal.



Figure 3 is a repeat of the experimental data in figure 2 with the exception that the data observed is a result of out-of-plane (OOP) 0.3mm pencil lead breaks made on the top edge of the panel. Data in figure 2 was made with 0.5mm lead breaks which give approximately twice the signal strength of 0.3mm leads. At the time the data was taken in figure 2, I was temporally out of 0.3mm pencil leads.

There are several interesting observations one can make when comparing the data in figure 3 for OOP sources as opposed to the IP data in figure 2. First note that there is a lack of the extensional wave component at this amplification in Figure 3 for the small aperture SE1000-HI and only faint evidence of this wave in the data from the SE9125-MI. Secondly the shear wave component is observed in all of the signals in figure 3 as well as in figure 2. Third, the zero order antisymmetrical lamb wave (flexure wave) is the predominate feature of the data from the SE1000-HI in figure 3. Fourth, note the change of vertical scale between the data for the SE1000-HI and the SE9125-M in figure 3. The SE1000-HI, a small aperture mass loaded transducer is much more sensitive to large displacements produced by a flexure wave, while the larger aperture partially mass loaded SE9125-M has greater sensitivity than the SE1000-HI to extensional and shear waves.. Sixth, previous reports have shown that splitting the signals from the output of the SE9125-M into a low and high frequency components and taking the ratio of the high frequency/low frequency peak voltages resulted in voltage ratios of less than one for OOP sources and greater than one for IP sources for experiments conducted on steel bars. The data in figures 2 and 3 confirm that these ratios are also valid for this composite panel.

I was confident that the extensional and shear waves recorded in these experiments were propagating in the panel adhesively bonded to the honeycomb structure which the trigger and data transducer were mounted on. I was not so certain that the low frequency flexure wave was propagating in this panel alone. I was also interested in determining if a transducer mounted on one panel could detect IP and OOP waves that might be generated in the panel on the other side of the honeycomb structure. The following experiment was performed to answer these questions. Data was taken for the condition of the trigger and data transducer mounted on the same panel for IP and OOP signals. The data transducer was left in place and the trigger transducer was moved to the opposite panel, and pencil lead breaks were made adjacent to the trigger transducer. The SE9125-MI transducer was used for the IP experiment since it has a much better response for this type of signal. The SE1000-HI was used for the OOP experiment since it has much better response to this type of signal. Figure 4 shows the results of this experiment.



Note from the SE9125-MI results that moving the source and trigger transducer to the bottom plate, while leaving the data transducer in place, results in approximately 10dB of attenuation and a slight time delay. This time delay corresponds to the amount of time it takes for the signal to travel through the honeycomb structure to the top panel.

Note from SE1000-HI that there is no attenuation of the OOP signal when the source and trigger transducer are moved to the bottom panel. In fact this signal is higher amplitude than when source and trigger sensor were on the same panel as the data transducer. I ascribe this difference in amplitude to the lack of exact repeatability of the source input when breaking pencil leads. Note that the two signals are 180 degrees out of phase. The lack of attenuation and the 180 degree phase shift are positive evidence that the whole structure rather than a single panel is sustaining the low frequency flexure wave due to the OOP source.

In previous reports I have shown that a SE1000-HI mounted on a 1/4 inch diameter stainless steel rod with a pointed end, could be used effectively in detecting very small displacements in metal bars. This experiment was repeated in this work on the graphite-epoxy panel. An aluminum cylinder 1.5 inch in diameter and 2 inches long with a 1/4 inch diameter hole was used to support the waveguide in the vertical direction (figure 1). The waveguide transducer combination was placed 8 inches from OOP 0.3mm pencil lead breaks and lead breaks were made on the top and bottom surface of the panel. The waveguide transducer was always positioned on the top panel, but the trigger transducer was placed at the location of the pencil lead breaks. No couplant was used between the tip of the waveguide and panel.

Figure 5 shows the results of this experiment. A lot of "ringing" of the signal occurs due to reflections in the wave guide, but the sensitivity and phase information (notice the 180 degree phase shift for the two conditions) is maintained.

DISCUSSION OF RESULTS

There were three types of waves observed in this panel during the course of these experiments: extensional and shear waves in the top and bottom cover plates, and a low frequency flexure wave in the honeycomb panel as a whole. Each of these waves travels at a different velocity. It was found that at least 8 inches between the source and transducer was required in order to get good time separation of the three different wave types. The SE9125-MI data for the 8 inch distance shown in figure 3 is a good example of the three types of waves present. Note that the peak voltage of the high frequency shear wave is approximately the same value as the low frequency flexure wave for this OOP signal. This transducer was designed to produce a voltage ratio of 1 or less for these two frequency components for OOP signals based on experiments on metal bars. It appears that this feature also is valid the composite specimen used in these experiments. Note that the ratio of high frequency/low frequency (HF/LF) in figure 2 from the SE9125-MI for IP signals is much greater than 1. Therefore one should be able to identify whether or not an AE signal is due to fiber breaking or matrix cracking (IP sources) as opposed to delamination, impact or friction (OOP) sources by simply looking at the peak voltage ratio (HF/LF) from the SE9125-MI.

This could have important implications for monitoring of space vehicles constructed from composite materials. For example assume that a composite tank is used in a space vehicle to carry liquid hydrogen, and one wishes to use AE to determine if meteorite impacts occur and if so, has any damage occurred. A meteorite impact would act as an OOP source and a SE9125-MI mounted to the pressure vessel would read a HF/LF ratio of 1 or less. If the meteorite penetrates the shielding and impacts on the composite pressure vessel and causes fibers to be broken, a HF/LF ratio of greater than 1, indicating an IP source will be produced which indicates that damage has occurred. Once an IP source has been identified assessment of the damage can estimated by the energy, amplitude, or counts of the AE signal produced by the IP source. The risetime of the AE signals produced by IP sources (figure 2) is quite sharp and conventional time of arrival from several transducers could be used to accurately locate the source. The IP signals in figure 2 were produced by breaking pencil leads at the center edge of the panel and due to symmetry very little flexure wave component was produced. In real life the signals will not be produced at the exact center of the panel, and therefore some flexure wave component will be present and will arrive at a later time. The SE9125-MI is designed such that for an IP signal the higher frequency faster traveling wave will always be of higher amplitude than the slower flexure wave and will prevent inaccuracies in measuring time of arrivals encountered with standard AE transducers. One would have problems locating IP sources in the conventional way from signals produced by the high fidelity SE1000-HI. Note in figure 1 that the extensional wave produced by this transducer is much lower in amplitude than the following wave forms and thus could produce large time difference errors if one triggered on the extensional wave from one transducer and the flexure wave from another. Time difference errors in locating OOP sources with the SE9125-MI are significantly reduced due to the fact that the slower flexure wave is approximately the same amplitude as the faster wave (figure 3). This is not the case for the SE1000-HI (figure 3). The low frequency flexure wave produced by OOP sources can be detected very well with the pointed waveguide configuration (figure 5). This zero aperture configuration is not well suited for detecting IP sources. In our space application example, if one were only interested in measuring and locating impacts from meteorites, this system could be used for this purpose. The advantage in using this type of configuration is that the transducer and associated electronics would be protected from the large thermal fluctuations that occur if bonded directly to the pressure vessel.

Both the SE9125-MI and the SE1000-HI have frequency response up to 1 Mhz. The instrumentation bandwidth used in these experiments were 20Khz to 1Mhz. FFT frequency analysis was performed on signals from both transducers. The frequency components above 200Khz were negligible compared to those below 200Khz. From a practical standpoint it appears that it makes no sense to attempt to use high frequency transducers and instrumentation for monitoring structures of this type of material because of the high attenuation in the high frequency range. Use of higher frequencies might be beneficial for small coupon testing in the laboratory, but it will be difficult to translate any information gained to practical field applications.

CONCLUSIONS

Acoustic Emission testing of the graphite-epoxy panel in this experimental yielded the following information. 1. The panel is anisotropic in that a 10% difference in velocity was observed between 0 and 90 degrees. For berivity only data in one direction was presented in this report. 2. The extensional and shear velocity in the panel was 5000m/sec and 1,330 m/sec respectively. 3. Attenuation for extensional waves was 0.1dB/mm and for flexure waves 0.05dB/mm. 4. OOP pencil lead breaks resulted in a low frequency flexure wave propagating in the whole panel including the honeycomb portion. This shows that it makes no difference which side of the panel a transducer is located on for detecting this type of signal. Approximately 10dB of attenuation was observed for extensional waves when the IP source is on the bottom panel and the transducer is on the top panel. 5. The SE9125-MI transducer was equally sensitive to both IP and OOP generated signals. 6. The AE signals had very little frequency content above 200Khz for transducer spacing used in these experiments. 7. A pointed waveguide mounted on a SE1000-HI could be used for detecting flexure waves due to OOP sources on either the bottom or top panel with very little attenuation when compared to the transducer mounted directly on the panel. 8. A shear wave was always detected by the SE9125-MI for both IP and OOP source inputs.